Q&A

(2019) Question 38: What are your guidelines for cleanliness of reactor vessel and overhead lines during Turnaround?  Do you have limits on reactor temperatures during dry-out to prevent the ignition of coke in the reactor?  What actions do you take if coke starts to burn?

What are your guidelines for cleanliness of reactor vessel and overhead lines during Turnaround?  Do you have limits on reactor temperatures during dry-out to prevent the ignition of coke in the reactor?  What actions do you take if coke starts to burn?

(2019) Question 39: What are your best practices for transferring FCC catalyst into/from pneumatic trailers and rail cars to ensure personnel safety and catalyst containment?

These trailers are often referred to as pneumatic, dry bulk, or pressure differential (PD) trailers. On-road trailers and railcars have similar functionality although railcars are not usually rated for vacuum, nor do they usually have a filter system. Both types of transport vessels have multiple hoppers.

(2019) Question 43: What are your best practices when shipping ecat, fines, feed, and slurry to suppliers for testing?  Please also comment on some best practices for sampling equilibrium catalyst.

When shipping ecat or fines, an appropriate sample container should be used. Catalyst suppliers will typically provide refiners with sample containers if needed. Catalyst shipping containers should be made of plastic or metal.

(2019) Question 44: What is your recommended back up options for slide valve / plug valve Hydraulic Power Units? Are electric actuators an option? What are the response times?

What is your recommended back up options for slide valve / plug valve Hydraulic Power Units? Are electric actuators an option? What are the response times?

(2018) Question 44: Describe your procedures for placing and operating the FCC in hot standby/safe park mode. What safety concerns do you consider and what safeguards should be in place?

If the air blower is not running, things you should consider are ensuring all ignition sources are shutdown, bypassed or isolated (ESP, torch oil, DFAH, CO Boiler). Verify all hydrocarbon sources to the reactor, riser and regenerator are closed (fresh feed, any recycles, torch oil, fuel gas purges, LCO quench, etc.) and all sources of air are not being injected (main air, plant instrument air, fluffing air, etc.).

(2018) Question 45: What are the safe and reliable options for rodding out plugged bleeders such as hydraulic ram pumps, packing gland / drill assemblies or tangential bleeders? How are these options used in a best practice for ensuring piping is hydrocarbon free and ready for maintenance?

Rod out tools or bleeder cleaners are safe and effective at clearing clogged drain, vent and instrument valves to be cleaned during normal operations. Most include some type of drill bit and local pressure gauge and are designed to handle high temperature and pressure applications.

(2018) Question 52: What are your best practices for wet flue gas scrubber water supply and system monitoring (sampling frequency, instrumentation verification, etc.)? How do you handle the effluent water and any new emerging trends?

Water supply should be managed depending on the system design. The water source used by Motiva is clarified water. Due to the stainless-steel material and the chloride concentration in both the water and the caustic for neutralization the inlet duct temperature is monitored and controlled to prevent Chloride Stress Corrosion Cracking.

(2017) Question 3: What are your Best Practices for unloading solid phosphoric acid (SPA) catalyst from a catalytic polymerization unit, and what safety issues do they address?

There are two types of Honeywell UOP Cat Poly reactors: chamber and tubular. Each has different unloading concerns, and there are several different unloading options available for each.

(2017) Question 4: For the isomerization unit, what is your treatment for the streams containing high concentrations of hydrochloric acid (HCl) in the reactor emergency depressurization system?

Honeywell UOP does not include treatment of gas from the reactor effluent as it enters the flare header when using the emergency depressuring system in our Penex™ and Butamer™ process unit designs.

(2017) Question 5: Is the presence of pyrophoric compounds common in feed/effluent exchangers? What neutralization methods do you employ prior to exposing the equipment to the atmosphere?

In 2015, UOP led a Principles & Practices session on the topic of NHT (naphtha hydrotreater) and reforming unit feed/effluent exchanger fouling and cleaning.

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