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(2017) Question 58: What are your Best Practices for reliably measuring level in the bottom of the main fractionator?

The following tables list the demonstrated technologies to reliably measure main column bottoms (MCB) level. Regardless of the technology used, it is important to have redundant level indication. The Best Practice is to employ two level transmitters with a selector switch for MCB level control. For displacers, guided-wave radar, and dP level transmitters, redundant transmitters should be on independent vessel taps. There are benefits to having two different level technologies employed. For point level measurement, at least two points should be measured for high and low levels.
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(2017) Question 73: Gasoline octanes continue to have a high value for many refineries. What fractionation strategies do you apply to increase gasoline octane? What rules of thumb do you apply for estimating changes in octane with gasoline endpoint adjustments?

RVP and endpoint both have a minor effect on gasoline octane. With other operating parameter changes and repeatability of octane results in the lab (+/- 0.5 RON), it is difficult to quantify small changes in octane caused by fractionation changes. Literature suggests that for every 1.5 psi RVP increase, RON will increase 0.3. We have very little data to support the literature, because the octane and RVP value of mixed C4s is much greater as alkylate than on the frontend of FCC gasoline.
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(2017) Question 74: How do you mitigate aqueous corrosion in the main fractionator overhead and gas concentration unit? What contaminants do you test for in the sour water, and what limits do you impose? What are your concerns with using stripped sour water as waterwash?

Over the last six years, there have been a number of questions related to different aspects of overhead and gas concentration unit corrosion management, including design recommendations. For completion of the Answer Book, here is a brief summary of the topics covered.
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(2017) Question 75: What are your Best Practices in design and operation to achieve positive isolation of slurry/HCO equipment?

Technip’s practice is to specify gate valves with flushing connections at the base of the seat. To ensure positive isolation, the flushing connection can be used to remove any sediments that may be impact the contact of the gate with the seat. Another option is to orient the valve stem off of vertical in order to move the final seating location away from the low point, therefore reducing the chances of sediment to accumulate there.
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(2016) Question 7: How is propane content in the refrigeration loop optimized against the compressor capacity to minimize contractor temperature? Do you have a good process model to predict the optimum propane content?

There is an optimum propane concentration in the refrigerant that will allow the alkylation unit to operate at a maximum alkylate throughput when the unit is up against limitations of both the compressor and the reaction zone heat removal capability. That optimum concentration of propane will vary from unit to unit and can be different seasonally. It can also be different from night to day or if exchangers are fouled, etc.
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(2016) Question 38: What do you see for the future of ebullated bed technology considering changes in crude quality and availability?

With the worldwide requirement for higher conversion of residue into lighter, more valuable transportation fuels such as diesel remaining firmly in place, we very much see ebullated-bed (EB) residue hydrocracking building on its current trend as a bottom-of-the-barrel upgrading technology of choice going forward. Investment in this commercially proven, well-established technology is a way to increase complexity and ensure long-term survival in an increasingly volatile marketplace.
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(2016) Question 39: Please summarize the current status of slurry hydrocracking technology commercialization.

Slurry hydrocracking technology has been commercialized in China (VCC) and Italy (EST) in the past two to three years. Both facilities have demonstrated expected performance, including conversion and selectivity. The reliability of slurry hydrocracking is still an open question as these units have only been in operation for a short time. Additional VCC commercial units are scheduled for startup in the next 12 months.
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(2016) Question 41: What are the considerations you use for extending hydrogen plant catalyst life cycles (i.e., lower production rates, furnace tube failure, etc.)?

There are many parameters affecting the hydrogen plant catalyst life cycles, such as lower production rates, furnace tube failure, unplanned plant shutdowns, larger catalyst volumes, elevated energy consumption, and finite ZnO/S (zinc oxide/sulfur) capacity. Lower Production Rates will obviously result in longer catalyst lifetime due to a lower gas velocity over the catalyst.
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