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(2017) Question 58: What are your Best Practices for reliably measuring level in the bottom of the main fractionator?

The following tables list the demonstrated technologies to reliably measure main column bottoms (MCB) level. Regardless of the technology used, it is important to have redundant level indication. The Best Practice is to employ two level transmitters with a selector switch for MCB level control. For displacers, guided-wave radar, and dP level transmitters, redundant transmitters should be on independent vessel taps. There are benefits to having two different level technologies employed. For point level measurement, at least two points should be measured for high and low levels.
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(2017) Question 73: Gasoline octanes continue to have a high value for many refineries. What fractionation strategies do you apply to increase gasoline octane? What rules of thumb do you apply for estimating changes in octane with gasoline endpoint adjustments?

RVP and endpoint both have a minor effect on gasoline octane. With other operating parameter changes and repeatability of octane results in the lab (+/- 0.5 RON), it is difficult to quantify small changes in octane caused by fractionation changes. Literature suggests that for every 1.5 psi RVP increase, RON will increase 0.3. We have very little data to support the literature, because the octane and RVP value of mixed C4s is much greater as alkylate than on the frontend of FCC gasoline.
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(2017) Question 74: How do you mitigate aqueous corrosion in the main fractionator overhead and gas concentration unit? What contaminants do you test for in the sour water, and what limits do you impose? What are your concerns with using stripped sour water as waterwash?

Over the last six years, there have been a number of questions related to different aspects of overhead and gas concentration unit corrosion management, including design recommendations. For completion of the Answer Book, here is a brief summary of the topics covered.
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(2017) Question 75: What are your Best Practices in design and operation to achieve positive isolation of slurry/HCO equipment?

Technip’s practice is to specify gate valves with flushing connections at the base of the seat. To ensure positive isolation, the flushing connection can be used to remove any sediments that may be impact the contact of the gate with the seat. Another option is to orient the valve stem off of vertical in order to move the final seating location away from the low point, therefore reducing the chances of sediment to accumulate there.
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(2016) Question 7: How is propane content in the refrigeration loop optimized against the compressor capacity to minimize contractor temperature? Do you have a good process model to predict the optimum propane content?

There is an optimum propane concentration in the refrigerant that will allow the alkylation unit to operate at a maximum alkylate throughput when the unit is up against limitations of both the compressor and the reaction zone heat removal capability. That optimum concentration of propane will vary from unit to unit and can be different seasonally. It can also be different from night to day or if exchangers are fouled, etc.
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(2016) Question 68: What is your experience with processing raw crude in the FCC? What types of crude have you tried to process in the FCC? What are the yield impacts? Any corrosion issues associated with this mode of operation? What additional corrosion monitoring is needed?

I have not had any experience running raw crude directly into an FCC unit; however, I know there are refiners out there that do. Many refiners who are running a high percentage of tight oils into their crude units have found that there is typically a shortage of FCC feed, which has led to some of them charging tight oils straight into the FCC.
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(2016) Question 69: Our FCC unit is limited by coke burn and high regenerator temperatures. What catalyst and operational changes have you implemented to maximize the conversion of heavy feeds and increase the amount of resid we can process without running into our regenerator limits and increasing dry gas production?

Considering the stated goals and constraints, particularly being limited by regenerator temperature and coke-burning capacity, it will be necessary to reduce delta coke without significantly increasing the reactor heat demand.
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(2016) Question 70: What is your method for measuring naphthenic acid [TAN (total acid number)] in FCC feed? Is this method affected by VABP (volume average boiling point) or Concarbon (Conradson carbon) content? Do you have data that validates an appropriate integrity operating window (IOW) trigger level? If above the trigger level, what is your recommended corrective action (extra inspection, change crude/slate, etc.)?

In terms of TAN number, we typically recommend the standard test method UOP 565, which can be found through the ASTM (American Society for Testing and Materials) website.
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